Postdoctoral Researcher - Electrochemistry & Operando Interfacial Characterization (CNM)

The Center for Nanoscale Materials (CNM) at Argonne National Laboratory seeks a highly motivated postdoctoral researcher with deep expertise in electrochemistry. The successful candidate will lead efforts in nanomaterials synthesis and in situ/operando characterization of liquid–solid interfaces during electrochemical conversions. This position offers the opportunity to leverage CNM’s advanced user facilities and instrumentation, publish in high-impact venues, and collaborate closely with scientists across CNM, Argonne, and external partners. Key Responsibilities Design, synthesize, and rigorously evaluate well‑defined nanomaterials for catalytic and electrochemical applications. Develop, implement, and optimize in situ electrochemical cells to probe liquid–solid interfaces under reaction conditions. Plan and execute in situ/operando experiments using advanced characterization methods, including Near Ambient Pressure X-ray Photoelectron Spectroscopy (NAP‑XPS), electron microscopy, Raman spectroscopy, and related techniques. Conduct electrochemical testing and benchmarking; analyze and interpret complex datasets to elucidate mechanisms and structure–property relationships. Document results and lead preparation of manuscripts, reports, and presentations; present findings at internal meetings and external conferences. Collaborate in a multidisciplinary team environment spanning experimentalists, theorists/modelers, and data scientists. Position Requirements Recent or soon‑to‑be‑completed PhD (within the last 0‑5 years) in Materials Science, Chemical Engineering, Chemistry, or a closely related field. Demonstrated expertise in electrochemistry, including materials synthesis, electrochemical characterization, and mechanistic interpretation. Hands‑on experience with in situ/operando characterization techniques. Strong data analysis skills; familiarity with modeling and/or data‑science tools is beneficial but not required. Excellent written and verbal communication skills and the ability to work effectively in a collaborative research environment. Ability to model Argonne’s core values of impact, safety, respect, integrity, and teamwork. Job Family : Postdoctoral | Job Profile : Postdoctoral Appointee | Worker Type : Long‑Term (Fixed Term) | Time Type : Full time Salary : The expected hiring range for this position is $72,879.00–$121,465.00. Pay will be determined based on qualifications and market considerations. Comprehensive benefits are part of the total rewards package. As an equal employment opportunity employer, Argonne National Laboratory is committed to a safe and welcoming workplace that fosters collaborative scientific discovery and innovation. Argonne encourages everyone to apply for employment. Argonne is committed to nondiscrimination and considers all qualified applicants for employment without regard to any characteristic protected by law. #J-18808-Ljbffr Argonne National Laboratory